Inficon 3000 Micro GC Gas Analyzer Operating Manual Manual do Utilizador

OPERATING MANUAL3000 Micro GCGas AnalyzerPN 074-519-P1CCover Page

TOC - 2 PN 074-519-P1C3000 Micro GC Operating Manual3.2.2 3,4-Channel Chassis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 26PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.3.6 Install the Vent Tubing and Connect to PowerCAUTIONNever connect low and high pressure ve

5 - 27PN 074-519-P1C3000 Micro GC Operating Manual WARNINGKeep the power supply block away from gas inlets or other areas where gas may collect or lea

5 - 28PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.5 Heated Regulator/Vaporizer Part NumbersThe Heated Regulator and Heated Vaporizer are suppli

5 - 29PN 074-519-P1C3000 Micro GC Operating Manual G2846A-6 Australia/NZ Heated Vaporizer for gas sampling:3,4-chG2846A-7 Korea Heated Vaporizer for g

5 - 30PN 074-519-P1C3000 Micro GC Operating Manual5.2 The Remote ConnectorFor some applications, an external triggering device may be required for sa

5 - 31PN 074-519-P1C3000 Micro GC Operating Manual Figure 5-39 shows the remote start cable.Figure 5-39 G2801-60618 remote start cableFigure 5-40 sho

5 - 32PN 074-519-P1C3000 Micro GC Operating ManualTable 5-11 shows the remote start/cancel action matrix.5.2.1 EZ IQ Operation to Activate Remote Sta

5 - 33PN 074-519-P1C3000 Micro GC Operating Manual 5.3 Multi-Position Valve Installation and Setup3000 Micro GC can be equipped with a Valco (VICI) s

5 - 34PN 074-519-P1C3000 Micro GC Operating Manual5.3.2 Valve Hardware Connections1 Assemble the multiposition microelectric valve actuator and contr

6 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 6Instrument Setup ThroughEmbedded Web Page Operation6.1 Overview3000 Micro GC has an embedd

TOC - 3PN 074-519-P1C3000 Micro GC Operating Manual 4.1.3 Site Requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6 - 2PN 074-519-P1C3000 Micro GC Operating ManualThe information listed on the home page will contain: 3000 Micro GC serial number Number of GC modu

6 - 3PN 074-519-P1C3000 Micro GC Operating Manual 6.1.2 Determining 3000 Micro GC Advanced ConfigurationThe embedded web page displays detailed confi

6 - 4PN 074-519-P1C3000 Micro GC Operating Manual3 The 3000 Micro GC configuration is displayed. See Table 6-1 and Figure 6-5.Figure 6-5 Full system

6 - 5PN 074-519-P1C3000 Micro GC Operating Manual Codes for GC modules, sample pumps, and GC module layout are displayed in Figure 6-6.Figure 6-6 300

6 - 6PN 074-519-P1C3000 Micro GC Operating Manual6.2 Status6.2.1 Check GC Module ParametersWhen EZ IQ software is used to download a method, the inf

6 - 7PN 074-519-P1C3000 Micro GC Operating Manual 6.2.2 Check the Duty Cycle1 The duty cycle should be approximately 30 to 40% for column head pressu

6 - 8PN 074-519-P1C3000 Micro GC Operating Manual6.3.2 RestartTo restart the 3000 Micro GC:1 On the Utilities tab, click Restart. 2 A countdown scree

6 - 9PN 074-519-P1C3000 Micro GC Operating Manual 6.4 Change Carrier Gas ConfigurationThe type of carrier gas used for analysis can be changed throug

6 - 10PN 074-519-P1C3000 Micro GC Operating Manual4 Click Make Changes. See Figure 6-10.5 When prompted for a user name and password, type gasconfig f

6 - 11PN 074-519-P1C3000 Micro GC Operating Manual 8 Select the new carrier gas type from the drop-down list. See Figure 6-13.Figure 6-13 Selecting a

TOC - 4 PN 074-519-P1C3000 Micro GC Operating ManualChapter 5Accessory Installation5.1 Sample Conditioners . . . . . . . . . . . . . . . . . . . . .

6 - 12PN 074-519-P1C3000 Micro GC Operating Manual11 Click Continue from the 3000 Micro GC status view to implement the configuration change.12 Change

6 - 13PN 074-519-P1C3000 Micro GC Operating Manual 6.5 Change IP Address6.5.1 IP ConfigurationThe 3000 Micro GC IP address can be changed through th

6 - 14PN 074-519-P1C3000 Micro GC Operating Manual5 When prompted for a user name and password, type ipconfig for both. See Figure 6-19.Figure 6-19 I

6 - 15PN 074-519-P1C3000 Micro GC Operating Manual 7 A window will prompt to restart 3000 Micro GC. Click Restart and wait at least three minutes befo

6 - 16PN 074-519-P1C3000 Micro GC Operating Manual6.5.2 Access the Embedded Web Page Via a Fixed IP AddressIf the embedded web page cannot be accesse

6 - 17PN 074-519-P1C3000 Micro GC Operating Manual 4 On the Local Area Connection Status window, click Properties. See Figure 6-25.Figure 6-25 Local

6 - 18PN 074-519-P1C3000 Micro GC Operating Manual6 In the Internet Protocol (TCP/IP) Properties window, click Use the following IP address. See Figur

6 - 19PN 074-519-P1C3000 Micro GC Operating Manual 11 Click Start >> Run.12 Type ping 192.168.1.99.This will open the Command Prompt window. The

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7 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 7Basic EZ IQ Operation7.1 IntroductionEZ IQ is powerful chromatography software running und

TOC - 5PN 074-519-P1C3000 Micro GC Operating Manual Chapter 6Instrument Setup Through Embedded Web Page Operation6.1 Overview. . . . . . . . . . . .

7 - 2PN 074-519-P1C3000 Micro GC Operating Manual3 On the Instrument Configuration window, type the desired Instrument Name, select Instrument type: 3

7 - 3PN 074-519-P1C3000 Micro GC Operating Manual 5 Double-click the INFICON 3000 Micro GC icon in the Configured modules pane to open the INFICON 300

7 - 4PN 074-519-P1C3000 Micro GC Operating Manual7.3 Configuring EZ IQ to Use a Valco (VICI) ValveTo configure an EZ IQ data system to use a Valco (V

7 - 5PN 074-519-P1C3000 Micro GC Operating Manual 7.3.1 Configuring a Valco (VICI) Switching Valve1 The 3000 Micro GC Enhanced Driver window will dis

7 - 6PN 074-519-P1C3000 Micro GC Operating Manual4 Select the desired parameters. See Table 7-1 for a list of parameters.5 Click Set Config to set the

7 - 7PN 074-519-P1C3000 Micro GC Operating Manual 7.3.2 Configuring a Valco (VICI) Sampling Valve1 The 3000 Micro GC Enhanced Driver window will disp

7 - 8PN 074-519-P1C3000 Micro GC Operating Manual4 Select the desired parameters. See Table 7-2 for a list of parameters.Table 7-2 Valco (VICI) sampl

7 - 9PN 074-519-P1C3000 Micro GC Operating Manual 7.4 Navigating EZ IQWhen EZ IQ is opened, the Instrument Window will display. From this window, all

7 - 10PN 074-519-P1C3000 Micro GC Operating ManualBy default, a Navigation pane is displayed at the left side of the instrument window. This view enab

7 - 11PN 074-519-P1C3000 Micro GC Operating Manual 7.5 EZ IQ WorkflowThe following steps outline the workflow for EZ IQ. 1 Basic Method Development a

TOC - 6 PN 074-519-P1C3000 Micro GC Operating Manual7.10.2 Common Integration Events. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 12PN 074-519-P1C3000 Micro GC Operating Manual7.6 Basic Method DevelopmentA method is used whenever a data file is acquired and/or reprocessed. I

7 - 13PN 074-519-P1C3000 Micro GC Operating Manual 7.6.1 Creating a New MethodTo create a new method:1 Open EZ IQ 2 Click File >> Method >&g

7 - 14PN 074-519-P1C3000 Micro GC Operating Manual4 The Instrument Setup window will display parameters that can be changed. See Figure 7-17.NOTE: The

7 - 15PN 074-519-P1C3000 Micro GC Operating Manual 6 Click the Trigger tab and select the trigger Type for the type of remote start installed in 3000

7 - 16PN 074-519-P1C3000 Micro GC Operating Manual7.6.2 Opening a MethodTo open a method,1 Click File >> Method >> Open.2 The Open Method

7 - 17PN 074-519-P1C3000 Micro GC Operating Manual 7.6.3 Downloading a MethodWhen a new method is created, or when a method is changed or opened, it

7 - 18PN 074-519-P1C3000 Micro GC Operating Manual7.6.4 View Instrument StatusClick Control >> Instrument Status to view 3000 Micro GC status.

7 - 19PN 074-519-P1C3000 Micro GC Operating Manual 7.7 Run a SampleOnce a method has been downloaded to 3000 Micro GC, a data acquisition run can be

7 - 20PN 074-519-P1C3000 Micro GC Operating Manual7.8 Basic SequencingA simple way to sequence data runs is to change the Number of reps in the Singl

7 - 21PN 074-519-P1C3000 Micro GC Operating Manual 7.10 Integrating the ChromatogramEZ IQ provides integration of peaks for analysis of simple chroma

TOC - 7PN 074-519-P1C3000 Micro GC Operating Manual Chapter 8Instrument Operations8.1 Routine Operation . . . . . . . . . . . . . . . . . . . . . .

7 - 22PN 074-519-P1C3000 Micro GC Operating Manual7.10.2 Common Integration EventsFrequently used event parameters are explained below. See the 074-5

7 - 23PN 074-519-P1C3000 Micro GC Operating Manual 7.10.2.3 Integration OffThe Integration Off event turns off the integration of the chromatogram fr

7 - 24PN 074-519-P1C3000 Micro GC Operating Manual4 Set the integration Start Time, Stop Time, and Value as desired.5 To save the method, click File &

7 - 25PN 074-519-P1C3000 Micro GC Operating Manual 7.10.3.2 Graphically Programming Integration Events1 Right-click on the chromatogram and select th

7 - 26PN 074-519-P1C3000 Micro GC Operating Manual7.11 Qualify PeaksUse the following steps to qualify, or identify peaks.7.11.1 Annotate a Chromato

7 - 27PN 074-519-P1C3000 Micro GC Operating Manual 5 Click Available Annotation then select which features to annotate. For example, selecting Retenti

7 - 28PN 074-519-P1C3000 Micro GC Operating Manual7.11.2 Adding Peak and Group InformationPeaks and groups can be identified in several ways. The inf

7 - 29PN 074-519-P1C3000 Micro GC Operating Manual 7.11.2.2 Define Peaks Graphically1 Click the Define Single Peak icon on the Int Event toolbar. See

7 - 30PN 074-519-P1C3000 Micro GC Operating ManualFigure 7-38 Define single peak through graphical programmingThe Define Single Peak window will appe

7 - 31PN 074-519-P1C3000 Micro GC Operating Manual 4 Click Next >> to move to the next detected peak. Click << Back to move to the previou

TOC - 8 PN 074-519-P1C3000 Micro GC Operating Manual8.5.2 Battery Usage Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 32PN 074-519-P1C3000 Micro GC Operating ManualISTD ID# If an internal standard calibration will be performed, enter the ID # for the internal stan

7 - 33PN 074-519-P1C3000 Micro GC Operating Manual 7.11.2.3 Adding GroupsTo add a group:1 Click Method >> Peaks/Groups from the toolbar.2 Click

7 - 34PN 074-519-P1C3000 Micro GC Operating Manual7.11.3 Adjust Peak WindowsRetention time windows will appear as red lines above peaks in the chroma

7 - 35PN 074-519-P1C3000 Micro GC Operating Manual 2 A blue Adjust Retention Time Window window will display. Click on the desired retention time wind

7 - 36PN 074-519-P1C3000 Micro GC Operating Manual7.12 CalibrationA calibration must be performed to quantify a peak (i.e., determine the amount of a

7 - 37PN 074-519-P1C3000 Micro GC Operating Manual 7.12.3 Perform A Single Level CalibrationTo quantify unknown samples, the method must contain the

7 - 38PN 074-519-P1C3000 Micro GC Operating Manual2 The Analysis/Single Level Calibration window will display.Figure 7-48 Analysis/single level calib

7 - 39PN 074-519-P1C3000 Micro GC Operating Manual 8 Select the Calibration check box and type 1 for Calibration level. See Figure 7-50. NOTE: For the

7 - 40PN 074-519-P1C3000 Micro GC Operating Manual7.12.4 Perform a Multiple Level CalibrationIf a multiple level calibration is required, sample cali

7 - 41PN 074-519-P1C3000 Micro GC Operating Manual 7.12.5 Review CalibrationAfter completing a calibration, a calibration curve and associated data c

TOC - 9PN 074-519-P1C3000 Micro GC Operating Manual Chapter 10Service and Technical Support10.1 How to Contact Customer Support. . . . . . . . . . .

7 - 42PN 074-519-P1C3000 Micro GC Operating Manual7.13 Generate Standard ReportsEZ IQ provides various standard report templates, such as an External

7 - 43PN 074-519-P1C3000 Micro GC Operating Manual 7.13.1.1.1 Custom Method Report FeaturesA number of features in the Method Report window are outli

7 - 44PN 074-519-P1C3000 Micro GC Operating Manual7.13.1.1.2 Importing a Template File1 Right-click in the Method Report window.2 Select Import Repor

7 - 45PN 074-519-P1C3000 Micro GC Operating Manual 7.13.1.2 Save a Custom Method Report1 Once all desired information has been modified or added, rig

7 - 46PN 074-519-P1C3000 Micro GC Operating Manual7.13.1.3 View or Print a Custom Method Report1 To view the custom method report, click Reports >

7 - 47PN 074-519-P1C3000 Micro GC Operating Manual 7.13.2 External Standard (ESTD) ReportsAn ESTD Report contains information on retention time, area

7 - 48PN 074-519-P1C3000 Micro GC Operating Manual4 Click Save.5 Click Yes to overwrite the current file. See Figure 7-61.Figure 7-61 Save a customiz

7 - 49PN 074-519-P1C3000 Micro GC Operating Manual 7.14 EZ IQ Operation to Activate Remote Start/Cancel FunctionTo use the remote connector function

7 - 50PN 074-519-P1C3000 Micro GC Operating Manual7 Click Start to begin sample acquisition. The run queue will be pending until the REMOTE_START cont

7 - 51PN 074-519-P1C3000 Micro GC Operating Manual 8 To abort the remaining runs in the run queue during a run. Close the REMOTE_CANCEL contact, which

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7 - 52PN 074-519-P1C3000 Micro GC Operating Manual7.15 Apply the Valco Valve Program to EZ IQ Method7.15.1 Valco Valve Setup in EZ IQ1 In EZ IQ, cli

7 - 53PN 074-519-P1C3000 Micro GC Operating Manual 7.15.2 Running a Sample with a Valco Valve1 In EZ IQ, click Control >> Single Run to display

7 - 54PN 074-519-P1C3000 Micro GC Operating Manual7.15.3 Running a Sequence with a Valco ValveA sequence of multiple runs with different valve positi

8 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 8Instrument Operations8.1 Routine Operation8.1.1 System BakeoutOver time, small amounts of

8 - 2PN 074-519-P1C3000 Micro GC Operating ManualFigure 8-1 Example bakeout method3 Click File >> Method >> Save to save the bakeout meth

8 - 3PN 074-519-P1C3000 Micro GC Operating Manual 8.1.2 Shutdown/RestartCAUTIONAvoid shutting down 3000 Micro GC using the power switch on the front

8 - 4PN 074-519-P1C3000 Micro GC Operating Manual3 Click Control >> Instrument Status to display the EZ IQ Instrument Status screen. Wait until

8 - 5PN 074-519-P1C3000 Micro GC Operating Manual 8.2 Remove and Replace a 3000 Micro GC ModuleThe following procedure will outline the steps necessa

8 - 6PN 074-519-P1C3000 Micro GC Operating Manual8.2.3 Update the Instrument FirmwareBefore installing a new GC Module, the 3000 Micro GC firmware mu

8 - 7PN 074-519-P1C3000 Micro GC Operating Manual 8.2.4 Decommission a Standard GC ModuleA Standard GC module must be decommissioned within the embed

1 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 1IntroductionThis operating manual describes the use and maintenance of the INFICON 3000 Mic

8 - 8PN 074-519-P1C3000 Micro GC Operating ManualFigure 8-4 Change module configuration4 Two caution messages appear. Read the caution, then click OK

8 - 9PN 074-519-P1C3000 Micro GC Operating Manual Figure 8-6 Decommission a GC module - remove options7 Click Shutdown on the confirmation message. S

8 - 10PN 074-519-P1C3000 Micro GC Operating ManualFigure 8-8 Decommission a GC module - restart instrument countdown9 Set the 3000 Micro GC front pan

8 - 11PN 074-519-P1C3000 Micro GC Operating Manual 8.2.5 Remove a GC ModuleThe old GC Module must be physically removed from 3000 Micro GC before the

8 - 12PN 074-519-P1C3000 Micro GC Operating ManualFigure 8-9 Thumbscrews on manifold cover plate5 Carefully remove the manifold insulation. Save it f

8 - 13PN 074-519-P1C3000 Micro GC Operating Manual NOTE: In Portable 3000 Micro GC, the DC-DC converter assembly blocks access to the GC modules. Remo

8 - 14PN 074-519-P1C3000 Micro GC Operating Manual7 Disconnect the inlet manifold fitting from the GC module input fitting using a 1/4 in. open-ended

8 - 15PN 074-519-P1C3000 Micro GC Operating Manual Figure 8-15 Remove the GC module10 Inspect the gang block fitting on the bottom of the chassis to

8 - 16PN 074-519-P1C3000 Micro GC Operating Manual8.2.6 Install a GC ModuleOnce a module is removed, it can be replaced with another module. If the r

8 - 17PN 074-519-P1C3000 Micro GC Operating Manual 2 Remove the small metal plate covering the O-rings on the upper gang block. See Figure 8-19.Figure

1 - 2PN 074-519-P1C3000 Micro GC Operating ManualOnly clean gases or vapors should be introduced to 3000 Micro GC. Avoid aerosols, condensable vapors,

8 - 18PN 074-519-P1C3000 Micro GC Operating Manual4 Remove the protective 1/4 in. cap from the GC module inlet fitting. See Figure 8-21.Figure 8-21 G

8 - 19PN 074-519-P1C3000 Micro GC Operating Manual 7 Reconnect the communications cables. See Figure 8-23.NOTE: Do not connect more than two GC module

8 - 20PN 074-519-P1C3000 Micro GC Operating Manual8.2.7 Commission a New Standard GC ModuleFor Standard GC modules, a new module IP address must be a

8 - 21PN 074-519-P1C3000 Micro GC Operating Manual 7 Select the correct module address for the new standard GC module from the drop-down list (see Fig

8 - 22PN 074-519-P1C3000 Micro GC Operating ManualFigure 8-28 Commission a standard GC Module - restart instrument countdown10 Set the 3000 Micro GC

8 - 23PN 074-519-P1C3000 Micro GC Operating Manual 8.3 Sample Conditioners8.3.1 Sample Conditioner Connections There are multiple types of optional

8 - 24PN 074-519-P1C3000 Micro GC Operating Manual8.3.2 Running a Low Pressure, Clean Gas SampleTo obtain a low pressure, clean gas sample, use the s

8 - 25PN 074-519-P1C3000 Micro GC Operating Manual 8.3.3 Running a Low Pressure, Liquid/Particulate Containing Gas SampleFor gas samples containing l

8 - 26PN 074-519-P1C3000 Micro GC Operating Manual8.3.4 Running a High Pressure Gas Sample without Liquids/Particulates1 If the Pressure Reducer (PN

8 - 27PN 074-519-P1C3000 Micro GC Operating Manual 8.3.5 Running a High Pressure Gas Sample with Liquids/Particulates1 If the Pressure Reducer and Ge

1 - 3PN 074-519-P1C3000 Micro GC Operating Manual 1.2 Definition of Notes, Warnings and CautionsWhen using this manual, please pay attention to the N

8 - 28PN 074-519-P1C3000 Micro GC Operating Manual8.3.6 Running a High Pressure Gas Sample Containing C6+ ComponentsThis procedure is used for sample

8 - 29PN 074-519-P1C3000 Micro GC Operating Manual 6 Prepare the sample vessel.7 Connect the sample vessel to the quick disconnect fitting. Moderate p

8 - 30PN 074-519-P1C3000 Micro GC Operating Manual8.3.6.2 Using a Transfer Line or Other Continuous Sample Source1 The Heated Regulator accessory mus

8 - 31PN 074-519-P1C3000 Micro GC Operating Manual 6 Use EZ IQ software to load the desired method.7 Turn on the Heated Regulator.8 Wait approximately

8 - 32PN 074-519-P1C3000 Micro GC Operating Manual8.3.7 Running a High Pressure Liquid Petroleum Gas SampleThis procedure applies to high pressure LP

8 - 33PN 074-519-P1C3000 Micro GC Operating Manual 2 Turn 3000 Micro GC on.3 Wait three minutes until 3000 Micro GC has fully powered up.4 Use EZ IQ s

8 - 34PN 074-519-P1C3000 Micro GC Operating Manual14 Turn the relief valve toward Vent to release the back pressure in the system, then close the valv

8 - 35PN 074-519-P1C3000 Micro GC Operating Manual 8.4 Consumable Replacement Procedures8.4.1 Replacing the External 10 Micron Sample Inlet Filter D

8 - 36PN 074-519-P1C3000 Micro GC Operating Manual8.4.2 Replacing the 2 Micron Filter in the Heated Vaporizer (PN G2819A-X/G2846A-X/G2858A-X)The 2 mi

8 - 37PN 074-519-P1C3000 Micro GC Operating Manual 8.4.3 Replacing the 7 Micron Filter in the Heated Regulator (PN G2818A-X/G2845A/G2857A)The 7 micro

1 - 4PN 074-519-P1C3000 Micro GC Operating Manual1.3 Safety Overview3000 MicroGC meets IEC (International Electro-technical Commission) classificatio

8 - 38PN 074-519-P1C3000 Micro GC Operating Manual7 Remove the filter from the heater block.8 Disassemble the trap halves.9 To prevent potential leaks

8 - 39PN 074-519-P1C3000 Micro GC Operating Manual 8.5.2.1 To View the Battery StatusConnect to the Portable 3000 Micro GC embedded web page by enter

8 - 40PN 074-519-P1C3000 Micro GC Operating Manual8.5.2.3 Replace the BatteryTo replace the battery:1 Shutdown the 3000 Micro GC, refer to section 6.

8 - 41PN 074-519-P1C3000 Micro GC Operating Manual 10 Lift the battery pack to expose the wiring connections.10a Disconnect the positive (+) wires fro

8 - 42PN 074-519-P1C3000 Micro GC Operating Manual8.5.3 Onboard Carrier Gas SupplyThe onboard carrier gas cylinder connects to the Portable 3000 Micr

8 - 43PN 074-519-P1C3000 Micro GC Operating Manual 8.5.3.1 Refill Onboard Carrier Gas CylinderPortable 3000 Micro GC contains a refillable, high pres

8 - 44PN 074-519-P1C3000 Micro GC Operating ManualProceed as follows:1 Connect the Carrier Gas Cylinder Recharge Kit (PN PNU-2058) to the supply tank

8 - 45PN 074-519-P1C3000 Micro GC Operating Manual 7 Turn the needle valve on the Carrier Gas Cylinder Recharge Kit clockwise until closed. 8 If the c

8 - 46PN 074-519-P1C3000 Micro GC Operating Manual17 Set gas delivery pressure and check for leaks. See Table 8-5.8.5.3.2 Before Turning Off the Carr

9 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 9Troubleshooting9.1 Symptom, Cause, and Remedy TablesThe following tables identify common s

1 - 5PN 074-519-P1C3000 Micro GC Operating Manual WARNING3000 Micro GC has inlets which can be heated to 140°C. Touching the inlets once they are at o

9 - 2PN 074-519-P1C3000 Micro GC Operating ManualPoor sensitivity (continued) Impure carrier gas Ensure the carrier gas purity is between 99.995% and

9 - 3PN 074-519-P1C3000 Micro GC Operating Manual Chromatograms not separating/no data is showing3000 Micro GC requires power cycleRestart 3000 Micro

9 - 4PN 074-519-P1C3000 Micro GC Operating ManualInverted peaks;large, broad humps in chromatogramIncorrect carrier gas Check the carrier gases and en

9 - 5PN 074-519-P1C3000 Micro GC Operating Manual 9.1.2 Common Software ProblemsTable 9-2 Common software problemsSymptom Cause RemedyMethod grayed

9 - 6PN 074-519-P1C3000 Micro GC Operating ManualTCD and columns turn off (continued)High carrier gas pressure Ensure the carrier gas is supplying at

9 - 7PN 074-519-P1C3000 Micro GC Operating Manual TCD detector 'fault' (continued)Malfunctioning column or injectorCheck the flow coming out

9 - 8PN 074-519-P1C3000 Micro GC Operating Manual9.1.3 Common Connection ProblemsTable 9-3 Common connection problemsSymptom Cause Remedy3000 Micro

9 - 9PN 074-519-P1C3000 Micro GC Operating Manual 9.1.4 Common Hardware ProblemsTable 9-4 Common hardware problemsSymptom Cause RemedyOne carrier ru

9 - 10PN 074-519-P1C3000 Micro GC Operating Manual9.2 Common Chromatographic and Method ProblemsThis section will provide some guidance to help diagn

9 - 11PN 074-519-P1C3000 Micro GC Operating Manual 9.2.1.1.2 Baseline Wander and DriftBaseline wander or drift is to be expected when a flow or tempe

1 - 6PN 074-519-P1C3000 Micro GC Operating ManualCAUTION - Static Sensitive DeviceElectrostatic discharge (ESD) is a threat to electronics. Electrosta

9 - 12PN 074-519-P1C3000 Micro GC Operating Manual9.2.1.1.3 Baseline NoiseNoise is a continuous rapid baseline fluctuation, broadening the baseline a

9 - 13PN 074-519-P1C3000 Micro GC Operating Manual 9.2.1.2 Retention Time Symptoms9.2.1.2.1 Retention Time DriftRetention time drift is a steady inc

9 - 14PN 074-519-P1C3000 Micro GC Operating Manual9.2.1.3 Peak Symptoms9.2.1.3.1 No PeaksPossibilities include operator error, insufficient Sample P

9 - 15PN 074-519-P1C3000 Micro GC Operating Manual 9.2.1.3.3 Extra PeaksExtra (ghost) peaks are peaks that appear during a blank run, and peaks that

9 - 16PN 074-519-P1C3000 Micro GC Operating Manual9.2.1.4 Deformed peaksThe ideal chromatography peak is a pure Gaussian shape. In reality, some asym

9 - 17PN 074-519-P1C3000 Micro GC Operating Manual 9.2.1.4.3 Deformed Peak ApexTop (apex) of the peak is deformed.Figure 9-3 Deformed apexA deformed

9 - 18PN 074-519-P1C3000 Micro GC Operating Manual9.2.2 Method ProblemsThis section describes how to troubleshoot a method and solve problems that ar

10 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 10Service and Technical Support10.1 How to Contact Customer SupportWorldwide support is av

10 - 2PN 074-519-P1C3000 Micro GC Operating Manual10.4 Service ContractINFICON offers service contracts for an out-of-warranty 3000 Micro GC. INFICON

11 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 11Replacement Parts and GasesThis chapter lists the replacement part numbers (PN) for 3000

1 - 7PN 074-519-P1C3000 Micro GC Operating Manual 1.4 Electromagnetic Compatibility3000 Micro GC complies with the requirements of CISPR 11 and EN 61

11 - 2PN 074-519-P1C3000 Micro GC Operating ManualTable 11-1 Power cord descriptions and PNsDescription Part Number1 Power Cord for PN G2801-60746/60

11 - 3PN 074-519-P1C3000 Micro GC Operating Manual 11.2 GC ModulesThe GC module assembly contains the injector, column, column heater, detector, and

11 - 4PN 074-519-P1C3000 Micro GC Operating Manual11.2.2 Standard ModulesStandard modules have a two digit numerical ending based on column parameter

11 - 5PN 074-519-P1C3000 Micro GC Operating Manual 11.2.3 Standard Modules TableTo order a replacement Standard GC module, contact INFICON with the N

11 - 6PN 074-519-P1C3000 Micro GC Operating ManualG2801-60538 GCMOD-19 G2801-69015 Variable Vol. OV-1,1.2 µm 8 m G2801-60539 GCMOD-20 G2801-69016

11 - 7PN 074-519-P1C3000 Micro GC Operating Manual G2801-60644 GCMOD-41 G2801-69644 Variable Vol. PLOT-Q 8 m G2801-60649 GCMOD-42 G2801-69649 Vari

11 - 8PN 074-519-P1C3000 Micro GC Operating ManualG2801-60859 GCMOD-63 G2801-69859 1.0 µL BackFlush Stabilwax 14 m Stabilwax 1.2 m G2801-60860 G

11 - 9PN 074-519-P1C3000 Micro GC Operating Manual 11.2.4 Performance Enhanced ModulesPerformance Enhanced modules have a two digit alphabetic ending

11 - 10PN 074-519-P1C3000 Micro GC Operating Manual11.2.5 Performance Enhanced Modules TableTo order a replacement GC module, contact INFICON with th

11 - 11PN 074-519-P1C3000 Micro GC Operating Manual G2807-60541 GCMOD-FV G2807-69018 Variable Vol. Alumina 0.32 mm 10 m G2807-60542 GCMOD-FW G280

1 - 8PN 074-519-P1C3000 Micro GC Operating ManualThis page is intentionally blank.

11 - 12PN 074-519-P1C3000 Micro GC Operating ManualG2807-60694 GCMOD-GW G2807-69694 1.0 µL BackFlush OV-1, 2.0 µm 8 m Stabilwax 1.2 m G2807-60696

11 - 13PN 074-519-P1C3000 Micro GC Operating Manual G2807-61109 GCMOD-HW G2807-69044 0.4 µL BackFlush Alumina 0.25 mm 14 m Alumina 0.25 mm 1 m G280

11 - 14PN 074-519-P1C3000 Micro GC Operating Manual11.2.6 Discontinued Module Replacement IPNsDiscontinued GC modules are listed for service support

11 - 15PN 074-519-P1C3000 Micro GC Operating Manual 11.3 Sample Accessories and Filters11.3.1 Sample Conditioners* The Heated Regulator and Heated V

11 - 16PN 074-519-P1C3000 Micro GC Operating Manual11.3.2 Filters11.3.3 Other Support PartsTable 11-6 FiltersDescription Part Number7 Micron Partic

11 - 17PN 074-519-P1C3000 Micro GC Operating Manual 11.4 Checkout Gases11.4.1 Universal Checkout GasUniversal Checkout Gas may be used during instal

11 - 18PN 074-519-P1C3000 Micro GC Operating Manual11.5 NGA Checkout GasThe Natural Gas Analyzer (NGA) Checkout Gas may be used during installation o

11 - 19PN 074-519-P1C3000 Micro GC Operating Manual 11.5.1 RGA Checkout GasRefinery Gas Analyzer (RGA) Checkout Gas may be used during installation o

11 - 20PN 074-519-P1C3000 Micro GC Operating ManualThis page is intentionally blank.

2 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 2Specifications2.1 3000 Micro GC SpecificationsTable 2-1 Specifications1 or 2-channel 3000

2 - 2PN 074-519-P1C3000 Micro GC Operating Manual2.2 Environmental ConditionsThe following specifications are applicable to the 3000 Micro GC Heated

2 - 3PN 074-519-P1C3000 Micro GC Operating Manual 2.3.5 RepeatabilityTypical results for Relative Standard Deviation (RSD) at constant temperature an

www.inficon.com [email protected] ©2013 INFICONOPERATING MANUALPN 074-519-P1CTitle Page3000 Micro GCGas Analyzer

2 - 4PN 074-519-P1C3000 Micro GC Operating Manual2.3.10 Safety and Regulatory StandardsConforms to the following safety standards: CSA/National Reco

3 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 3Overview3.1 Overview of 3000 Micro GC Instrument and Accessories3000 Micro GC is a gas ana

3 - 2PN 074-519-P1C3000 Micro GC Operating Manual3.2 3000 Micro GC ChassisThere are three types of 3000 Micro GC chassis that house GC modules: 1,2-

3 - 3PN 074-519-P1C3000 Micro GC Operating Manual 3.2.2 3,4-Channel Chassis The 3,4-channel chassis can accept three or four channels. The carrier ga

3 - 4PN 074-519-P1C3000 Micro GC Operating Manual3.2.3 Portable Chassis Portable 3000 Micro GC is a completely self-contained, miniaturized gas chrom

3 - 5PN 074-519-P1C3000 Micro GC Operating Manual 3.3 The 3000 Micro GC Module3000 Micro GC utilizes a modular GC platform, which can simultaneously

3 - 6PN 074-519-P1C3000 Micro GC Operating Manual2 Separation: As the sample gas enters the column, its component gases are separated based on their r

3 - 7PN 074-519-P1C3000 Micro GC Operating Manual 3.3.2 Injector Flow AssemblyThe injector flow assembly (see Figure 3-10) consists of: MEMS injecto

3 - 8PN 074-519-P1C3000 Micro GC Operating Manual3.3.3 InjectorsDepending on application requirements, 3000 Micro GC supports four different types of

3 - 9PN 074-519-P1C3000 Micro GC Operating Manual 3.3.3.3 Fixed InjectorFixed Injectors are unique to 3000 Micro GC. Fixed Injectors provide the best

TrademarksThe trademarks of the products mentioned in this manual are held by the companies that produce them.3000 Micro GC™, Bring the Lab to the Sam

3 - 10PN 074-519-P1C3000 Micro GC Operating Manual3.3.3.4 Backflush InjectorThe backflush assembly consists of: a backflush injector a precolumn a

3 - 11PN 074-519-P1C3000 Micro GC Operating Manual 3.3.4 Columns3000 Micro GC utilizes capillary columns for separation. Two types of capillary colum

3 - 12PN 074-519-P1C3000 Micro GC Operating Manual3.3.5 Detector3000 Micro GC uses a MEMS based TCD, which has a 240 nL internal cell volume. (See Fi

3 - 13PN 074-519-P1C3000 Micro GC Operating Manual 3.3.7 Module Cases3000 Micro GC supports two types of module cases, a standard module case and a M

3 - 14PN 074-519-P1C3000 Micro GC Operating Manual3.4 3000 Micro GC Chassis Components3000 Micro GC modules are installed into the 3000 Micro GC chas

3 - 15PN 074-519-P1C3000 Micro GC Operating Manual 3.4.2 C-BoardThe Communications Board, also known as the C-board is internally mounted on the side

3 - 16PN 074-519-P1C3000 Micro GC Operating Manual3.4.4 Sample PumpOne or two sample pumps are installed internally in 3000 Micro GC. There is no flo

3 - 17PN 074-519-P1C3000 Micro GC Operating Manual 3.4.5 Carrier Gas WeldmentThe carrier gas weldment connects the carrier gas to each module. It con

3 - 18PN 074-519-P1C3000 Micro GC Operating Manual3.4.6 Carrier Gas InletOne or two carrier gases can be configured with the carrier gas inlets locat

3 - 19PN 074-519-P1C3000 Micro GC Operating Manual 3.4.7 VentsAnalytical vents expel sample gas and carrier gas mixture from the sample side of the T

DECLARATION OF CONFORMITY This is to certify that this equipment manufactured by: INFICON Instruments ( Shanghai ) Co., Ltd

3 - 20PN 074-519-P1C3000 Micro GC Operating Manual3.4.8 Remote Control ModuleThe Remote Control Module allows an external control system to start 300

3 - 21PN 074-519-P1C3000 Micro GC Operating Manual 3.5 Sample ConditionersCAUTION3000 Micro GC is a gas-only analyzer!Extreme caution must be taken t

3 - 22PN 074-519-P1C3000 Micro GC Operating Manual3.6 EZ IQ Chromatography SoftwareEZ IQ is a powerful chromatography software running under the Micr

3 - 23PN 074-519-P1C3000 Micro GC Operating Manual 3.7 Product IdentificationEach 3000 Micro GC carries a configuration specific part number (PN:), s

3 - 24PN 074-519-P1C3000 Micro GC Operating Manual3.7.1 1,2-Channel and Portable 3000 Micro GC Part NumberingThe 1,2-channel 3000 Micro GC chassis an

3 - 25PN 074-519-P1C3000 Micro GC Operating Manual 3.7.2 3,4-Channel 3000 Micro GC Part NumberingThe 3,4-channel 3000 Micro GC chassis can be equippe

3 - 26PN 074-519-P1C3000 Micro GC Operating Manual3.7.4 Identification NumberEach instrument is uniquely identified by an identification number (ID:)

4 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 4Installation 4.1 Site PreparationBefore installation, make sure that the installation site

4 - 2PN 074-519-P1C3000 Micro GC Operating Manual4.1.3 Site Requirements4.1.3.1 Electrical RequirementsA standard 100 to 240 V(ac) electrical outlet

4 - 3PN 074-519-P1C3000 Micro GC Operating Manual 4.1.5 Gas and Regulator Requirements4.1.5.1 Carrier Gas and Regulator RequirementsA continuous, co

4 - 4PN 074-519-P1C3000 Micro GC Operating Manual4.2 Instrument Hardware Setup4.2.1 Unpacking the InstrumentVerify the contents of the order, includ

4 - 5PN 074-519-P1C3000 Micro GC Operating Manual 4.2.2.2 Configuration Dependent Parts4.2.2.2.1 1,2-Channel and 3,4-Channel 3000 Micro GC Specific

4 - 6PN 074-519-P1C3000 Micro GC Operating Manual4.2.3 Making Carrier Gas and Sample Inlet Connectors3000 Micro GC is equipped with a 1/8 in. carrier

4 - 7PN 074-519-P1C3000 Micro GC Operating Manual 4 Ensure that the front ferrule makes contact with the female fitting, slide the Swagelok nut over t

4 - 8PN 074-519-P1C3000 Micro GC Operating Manual4.2.4 Connecting the Carrier Gas4.2.4.1 Gas SafetyWARNINGGas cylinders present a hazard when not se

4 - 9PN 074-519-P1C3000 Micro GC Operating Manual 4.2.4.2 Connecting the Carrier Gas Particulate Filter1 Remove any shipping caps on 3000 Micro GC.2

4 - 10PN 074-519-P1C3000 Micro GC Operating Manual4.2.4.3 Setting the Gas PressureSet the carrier gas regulator as shown in Table 4-1.WARNINGNever fi

4 - 11PN 074-519-P1C3000 Micro GC Operating Manual 4.2.4.5 Connecting the Carrier Gas to the 3000 Micro GC1 Connect the carrier gases to the instrume

4 - 12PN 074-519-P1C3000 Micro GC Operating ManualFigure 4-7 Portable 3000 Micro GC, back view4 Set the carrier switch on the front of Portable 3000

4 - 13PN 074-519-P1C3000 Micro GC Operating Manual 4.2.5.2 Tools Required Two 7/16 in. wrenches, for the sample inlet filter assembly One 5/16 in.

WARRANTY AND LIABILITY - LIMITATION: Seller warrants the products manufactured by it, or by an affiliated company and sold by it, and described on the

4 - 14PN 074-519-P1C3000 Micro GC Operating Manual4.2.6 Power and Communication Cable Setup1 Connect the crossover cable (PN 5183-4649) between the c

4 - 15PN 074-519-P1C3000 Micro GC Operating Manual 4.3 Instrument Configuration Setup3000 Micro GC can be connected directly to the computer on a LAN

4 - 16PN 074-519-P1C3000 Micro GC Operating Manual4.3.2 IP Address ConfigurationThe IP address on the computer must be changed in order to communicat

4 - 17PN 074-519-P1C3000 Micro GC Operating Manual 4.3.3 Ping the InstrumentEnsure that the instrument is turned on and is fully booted up. On the co

4 - 18PN 074-519-P1C3000 Micro GC Operating Manual4.4 Chromatography Software Installation For an in-depth guide on installing and configuring EZ IQ,

5 - 1PN 074-519-P1C3000 Micro GC Operating Manual Chapter 5Accessory Installation5.1 Sample Conditioners 3000 Micro GC can be damaged by contaminants

5 - 2PN 074-519-P1C3000 Micro GC Operating ManualHeated Regulator for Sampling14 to 5516 kPa(2 to 800 PSI)Transfer line or high-pressure vesselC6+ com

5 - 3PN 074-519-P1C3000 Micro GC Operating Manual 5.1.2 Installing the 10 Micron Sample Inlet FilterFor instruction on installing the 10 micron sampl

5 - 4PN 074-519-P1C3000 Micro GC Operating Manual5.1.3.2 User Supplied Parts Fittings for vent tubing, if used Sample input tubing and fittings5.1.

5 - 5PN 074-519-P1C3000 Micro GC Operating Manual 6 Install the sample outlet tube into the output fitting on the Genie Filter Assembly. See Figure 5-

5 - 6PN 074-519-P1C3000 Micro GC Operating Manual8 While maintaining the alignment of the outlet tubing to the inlet fitting, tilt the bracket up and

5 - 7PN 074-519-P1C3000 Micro GC Operating Manual 11 Install one end of the sample inlet tubing, 1/4 in. nut, and front and back ferrules provided in

5 - 8PN 074-519-P1C3000 Micro GC Operating Manual5.1.4 Installing the Pressure ReducerThe Pressure Reducer (PN G2815A) provides a pressure reducing f

5 - 9PN 074-519-P1C3000 Micro GC Operating Manual 5.1.4.3 Installation Instructions for the Pressure Reducer1 Turn off 3000 Micro GC and allow the sa

5 - 10PN 074-519-P1C3000 Micro GC Operating Manual6 Align the Pressure Reducer bracket horizontally on the face of the 3000 Micro GC so that the end o

5 - 11PN 074-519-P1C3000 Micro GC Operating Manual 10 Install 1/8 in. sample input line to the top right Swagelok fitting on the accessory. See Figure

5 - 12PN 074-519-P1C3000 Micro GC Operating Manual5.1.5 Installing the Pressure Reducer and Genie Filter AssemblyThe Pressure Reducer and Genie Filte

5 - 13PN 074-519-P1C3000 Micro GC Operating Manual 5.1.5.3 Installation Instructions for the Pressure Reducer and Genie Filter Assembly1 Turn off 300

5 - 14PN 074-519-P1C3000 Micro GC Operating Manual6 Insert the outlet tube into the outlet fitting on the Genie Filter Assembly. See Figure 5-17. Tigh

5 - 15PN 074-519-P1C3000 Micro GC Operating Manual 8 When maintaining the alignment of the outlet tubing and the inlet fitting, tilt the bracket up an

TOC - 1PN 074-519-P1C3000 Micro GC Operating Manual Table Of ContentsTrademarksDisclaimerCopyrightDeclaration Of ConformityWarrantyChapter 1Introduc

5 - 16PN 074-519-P1C3000 Micro GC Operating Manual12 Remove the blue cap from the 1/8 in. NPT male input fitting and install a user-provided 1/8 in. f

5 - 17PN 074-519-P1C3000 Micro GC Operating Manual Figure 5-22 shows the Pressure Reducer and Genie Filter Assembly mounted on 3000 Micro GC.Figure 5-

5 - 18PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.1 Heated RegulatorThe Heated Regulator for natural gas (PN G2818A-X/G2845A-X/G2857A-X) is a s

5 - 19PN 074-519-P1C3000 Micro GC Operating Manual 5.1.6.1.1 Target AnalytesNatural gas typically consists of methane and a wide distribution of othe

5 - 20PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.2 Heated VaporizerThe Heated Vaporizer (PN G2819A-X/G2846A-X/G2858A-X) is used for high press

5 - 21PN 074-519-P1C3000 Micro GC Operating Manual 5.1.6.2.1 Heated Vaporizer Accessory ContentsFigure 5-25 Heated vaporizer accessory kit5.1.6.3 I

5 - 22PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.3.2 User Supplied Parts T20 Torx screwdriver 1/16 in. stainless steel tubing for low pressu

5 - 23PN 074-519-P1C3000 Micro GC Operating Manual 5.1.6.3.4 Installing the Transfer Line1 The sample outlet fitting on the heated sample introductio

5 - 24PN 074-519-P1C3000 Micro GC Operating Manual5.1.6.3.5 Mounting the Heated Sample Conditioners1 Add female nut, front ferrules and back ferrules

5 - 25PN 074-519-P1C3000 Micro GC Operating Manual Figure 5-32 Installing the heated sample instroduction accessory on 3000 Micro GC3 Tighten the 300