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Inficon HAPSITE Smart Plus Chemical Identification System Manual do Utilizador (586 páginas)


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Índice

Smart Plus

1

Disclaimer

4

Copyright

4

Warranty

11

Definition of

13

Table Of Contents

15

TOC - 3

17

TOC - 5

19

TOC - 7

21

TOC - 9

23

TOC - 13

27

Chapter 1

29

Introduction

29

1.3 Serial Number Location

31

1.4 Theory of Operation

31

1.5 Instrument Overview

32

1.6.1 Gas Chromatograph

33

1.6.2 Mass Spectrometer

35

1.6.3 Vacuum System

36

1.6.4 Electronic Systems

37

1.6.5 Software Systems

38

2.1 Ship Kit Packing Lists

39

Box 1 Contents

39

Box 2 Contents

40

Box 3 Contents

40

Box 4 and 5 Contents

40

2.3.1 Ship Kits Box 3 and 4

43

2.4 Basic Assembly

43

2.4.1 Attaching the Probe

44

2.4.4 Install Battery

48

2 - 11

49

2.5 Helpful Guidelines

50

2.6 HAPSITE Configurations

51

2 - 14

52

2 - 16

54

2 - 17

55

2 - 18

56

2.8 Service Module

57

2 - 20

58

2 - 22

60

2 - 23

61

2 - 24

62

2 - 25

63

2 - 26

64

2.9 SituProbe

65

2 - 28

66

2 - 29

67

2 - 30

68

2.10 Sample Collection Modes

69

2 - 32

70

2 - 33

71

Figure 2-54 Wrench tighten

71

2 - 36

74

Figure 2-59

75

2 - 38

76

2 - 39

77

2 - 40

78

2 - 41

79

2.11.1 Probe Nut Assembly

80

2 - 45

83

2 - 46

84

3 Finger tighten the nut

84

2.12 Batteries

85

2.12.2 Battery Charger

86

2 - 49

87

2 - 50

88

2.13 Portable Accessories

89

2.13.2 HAPSITE Backpack

90

20%. This will provide an

93

2 - 56

94

Chapter 3

95

Figure 3-3 Details Button

96

Figure 3-7 Survey Ready

99

Figure 3-8 Analyze Ready

99

Figure 3-9 Emergency Mode

100

Figure 3-10 Arrow Keys

100

Figure 3-12

101

IPN 074-472-P1C

102

3 - 10

104

3 - 11

105

Figure 3-19 Skip Cleanout

105

3 - 14

108

3 - 15

109

Figure 3-25 Preparing System

109

3 - 16

110

3.2.2 Show All

111

3.3 Survey Mode

111

3 - 18

112

3 - 19

113

Figure 3-32 Survey Ready

113

3 - 20

114

3 - 21

115

3 - 22

116

3 - 23

117

Figure 3-41 ANALYZE and STOP

117

3 - 26

120

See Figure 3-46

121

3 - 28

122

3 - 29

123

3 - 32

126

3 - 33

127

Figure 3-53 Arrow Keys

127

Figure 3-54 Select Results

127

3 - 34

128

3 - 35

129

3 - 36

130

3 - 37

131

Figure 3-61 CMPD ID

131

3 - 38

132

3 - 39

133

Figure 3-64 Viewing REPORTS

133

Figure 3-65 Summary Report

133

3 - 40

134

3 - 41

135

Figure 3-68 Type of Method

135

3.6 The Help Icon

136

3.7 The Info Icon

137

3 - 44

138

SYNONYMS. See Figure 3-73

139

3 - 47

141

3 - 48

142

3 - 49

143

Figure 3-81 IDLH Screen

143

3.7.1 System Parameters

144

3 - 51

145

Figure 3-84 Battery Icon

145

Figure 3-85 Carrier Gas Icon

145

3 - 52

146

3 - 53

147

Figure 3-89 NEG Button

147

3 - 54

148

3 - 55

149

Figure 3-91 Run AutoTune

149

3 - 56

150

3 - 57

151

Figure 3-94 GPS Icon

151

3 - 58

152

3 - 59

153

Figure 3-98 DATE TIME

153

Figure 3-99 NET Button

153

3.7.2 Accessories

154

3.8 EXIT Menu

155

3 - 62

156

3.8.1 Extended Standby

157

3 - 64

158

Figure 3-108

159

Portable Mode

161

Figure 3-112 HSS Analyze

162

3 - 69

163

3 - 70

164

3 - 71

165

Figure 3-117 Purge

165

3.9.1 Quick Reference SOP —

166

3.10 SituProbe

167

3 - 74

168

3 - 75

169

3 - 76

170

3 - 77

171

3 - 78

172

4.1 Wireless Option

173

4.1.1 Introduction

173

4.1.5 Wireless Range

178

4.1.6 Turning On the Radio

179

4 - 11

183

4.2 The MAIN Menu

184

4.2.1 Smart Interface

184

4 - 13

185

Figure 4-7 Smart Interface

185

4.2.2 Adjust Brightness

186

4 - 15

187

Figure 4-12 Scroll Bar

187

Figure 4-13 OK Button

187

Figure 4-14 Black Screen

187

4 - 16

188

4.3 Touch Screen Options

189

4 - 18

190

4 - 19

191

4 - 20

192

4 - 21

193

Figure 4-25 Disable Button

193

4 - 22

194

4.4 The USB Drive

195

4 - 24

196

4 - 25

197

Figure 4-32 Select Files

197

Figure 4-33 Copy Files

197

4 - 26

198

4 - 27

199

Figure 4-36 Accessories Icon

199

4 - 29

201

Figure 4-39 Progress Bar

201

4 - 30

202

4 - 31

203

Figure 4-42 Update From USB

203

4 - 32

204

4 - 33

205

4 - 34

206

Chapter 5

207

5.2 Survey Mode

208

Figure 5-3 AutoTune Complete

209

Figure 5-4 Run Button

209

Figure 5-6 Stop Button

210

Figure 5-8 Data Review Icon

211

5 - 10

216

5 - 11

217

Figure 5-15 Run Button

217

5 - 12

218

5 - 13

219

Figure 5-17 Sample Complete

219

Figure 5-18 Data Review Icon

219

5.5.1 Tri- Bed Concentrator

221

5.5.2 The Tenax Concentrator

221

Figure 5-21 Run Button

222

5 - 17

223

Figure 5-25 Headspace Needle

226

5 - 21

227

5 - 22

228

5 - 23

229

5 - 26

232

5 - 27

233

5 - 28

234

6.1 Introduction to Methods

235

6.1.1 Sensitivity

235

6.2 Survey Method

235

6.3 Analyze (GC/MS) Methods

241

Target Compound Library File

242

Chapter 7

243

7.2 AutoTune

244

Computer

245

7.3 Viewing a Tune Report

246

Figure 7-8 Tune Report

247

7.4 AutoTune Failure

248

7.5.1 Tool Bar

252

7.5.2 Tune Drop Down Menu

253

7 - 12

254

7 - 13

255

7.5.3 Tune Control Panel

256

7 - 15

257

7 - 16

258

7.5.4 Peak Scan Window

259

7.5.5 Full Scan Window

261

7 - 20

262

7 - 21

263

7 - 22

264

7 - 23

265

7 - 24

266

7.6 Performing Manual Tune

267

Figure 7-27 Plus IQ Icon

268

Figure 7-28 Manual Tune Icon

268

7 - 27

269

Figure 7-31 BPG Low

269

7 - 32

274

7 - 33

275

Figure 7-37 Save Tune Button

275

Figure 7-38 Tune Saved

275

7 - 34

276

Chapter 8

277

Plus IQ Software

277

Figure 8-11

283

8 - 10

286

8 - 11

287

8 - 12

288

Laptop Computer

289

Figure 8-20 Add HAPSITE

290

8 - 15

291

8 - 16

292

8 - 17

293

8 - 18

294

8 - 19

295

8 - 20

296

8 - 21

297

8 - 22

298

8.9 Access Levels

299

8 - 25

301

8.10 Plus IQ Controls

302

8 - 27

303

Figure 8-44 System Menu

303

8 - 28

304

8 - 29

305

8.12 HAPSITE Icons

306

8 - 31

307

8 - 32

308

Chapter 9

309

Data Review

309

9.3 Data Review Toolbar

313

9 - 10

318

9 - 11

319

9 - 12

320

9 - 13

321

9 - 14

322

9 - 15

323

9 - 16

324

9.6 Using the Zoom Function

325

9 - 18

326

9 - 19

327

Figure 9-17 Zoomed Spectrum

327

9 - 20

328

9 - 21

329

Figure 9-20 RIC Plot

329

Figure 9-21 NIST Icon

329

Figure 9-22 NIST Names Tab

329

Figure 9-23 NIST Name Entry

330

Figure 9-24 Top 10 Masses

330

9 - 23

331

9.8 NIST Library Searches

332

9 - 25

333

9.8.1 Searching Peaks

334

9 - 27

335

9 - 28

336

9 - 29

337

9.8.3 How To Access AMDIS

338

9 - 31

339

9 - 33

341

Figure 9-40 NIST Menu

341

9 - 34

342

9 - 35

343

Figure 9-42 NIST Database

343

9 - 36

344

9 - 37

345

9.10 Plus IQ Hot Keys

346

10.1.1 Method Files

347

10 - 2

348

10.1.2 Event Log Files

349

10.1.3 Data Files

349

10.1.4 Tune Files

350

10 - 5

351

10 - 6

352

10.1.5 Data Review

353

10 - 8

354

10 - 9

355

10.2.1 Method Files

356

10.2.2 Event Log Files

357

10.2.3 Data Files

358

10.2.4 Tune Files

358

10.2.5 Report Files

358

10 - 13

359

10 - 14

360

11.1 The Method Editor

361

11 - 2

362

11 - 3

363

11.2 Accessing Method Editor

364

11.3 Description Page

365

11.3.1 Full Scan Method

366

11.3.2 SIM Method

367

11 - 8

368

11.4 Startup Page

369

11 - 10

370

11 - 11

371

11.4.1 Headspace

372

11.4.2 SituProbe

373

11.5 Inlet Page

374

Figure 11-13

375

11.5.1 Inlet States

376

11 - 17

377

11 - 18

378

11 - 19

379

11 - 20

380

11 - 21

381

11 - 22

382

11.5.3 Use Internal Standard

383

11.5.4 Scan Events

383

11 - 24

384

11.6 Tune Page

385

11.6.1 Param Page

385

11.6.2 Report Page

385

11 - 26

386

11 - 27

387

11 - 28

388

11.7 Full Scan Page

389

11.8 SIM Page

390

11 - 31

391

11 - 32

392

11.8.2 SIM for Survey

393

11 - 34

394

11.9 Search Page

395

11 - 36

396

11 - 37

397

11 - 38

398

11 - 39

399

Figure 11-31 Analyze Region

399

Figure 11-32 The Libraries

399

11 - 40

400

11 - 41

401

11 - 42

402

11 - 43

403

11 - 44

404

11 - 45

405

11.10 Data Page

406

11 - 47

407

11 - 48

408

11.11 Summary Page

409

11.12 How to Create a Method

410

Figure 11-48

411

11 - 52

412

11 - 53

413

... button. See Figure 11-54

414

11 - 55

415

Figure 11-55 Choose Method

415

11 - 58

418

Chapter 12

419

Target Compound Methods

419

12.2.1 Method

420

12.2.2 Data Files

420

12.2.3 Peak Search

421

12.2.4 Analytes

422

12.2.5 Reports

422

12.2.6 Extracted Mass Peaks

423

12.2.7 Calibration

423

12.3.1 Method

424

12.3.2 Data Files

424

12.3.3 Peak Search

425

12.3.4 Analytes

425

12.3.5 Reports

425

12.3.6 Extracted Mass Peaks

426

12.3.7 Calibration

426

12.4 Display Function

427

12 - 10

428

12 - 11

429

12 - 12

430

12 - 13

431

12 - 14

432

12 - 15

433

12 - 16

434

12 - 17

435

12 - 18

436

12 - 19

437

12 - 20

438

13.1 Introduction

439

13.1.1 How the HSS Operates

440

13.1.3 HSS Indicators

441

13.1.4 Consumables Required

442

13 - 5

443

13.2.1 Powering on the HSS

444

13.2.2 Loading the Vials

445

13 - 8

446

13 - 9

447

13.2.4 Cycling the Vials

451

13.3 Maintenance of HSS

451

13 - 14

452

13 - 15

453

13.4 Shipping the HSS

456

13 - 19

457

13 - 20

458

14.1 SituProbe

459

14.2 Theory

459

14 - 3

461

14.5 Consumables

462

14.5.1 Compressed Nitrogen

462

14.6 Heated Zones

463

14.7 Valves and Sequences

464

14.7.1 Headspace

464

14.7.2 Purge

464

14.7.3 Dry Purge

465

14.8 SituProbe Operation

465

14.8.1 Headspace Creation

465

14.8.2 Purge Rate Adjustment

465

14.8.3 Method Events

466

14.9 Background Cleanup

467

14.9.1 Introduction

467

14.9.2 Cleanup Steps

467

14.10 Operating Tips

468

14.10.1 Reducing Background

468

14.10.2 Nitrogen Usage

468

14.11 Calibration Standards

469

14.11.1 Introduction

469

14.11.2 Standard Preparation

469

14.11.3 Calculations

471

14.12 Calibration Curves

471

14.13 Maintenance

472

14.13.1 Surface Cleaning

472

15.1 Introduction

475

15 - 2

476

15.3.1 Backup Batteries

477

15.3.2 MDP/Turbo Pump

477

15.3.3 Manifold Vent Valve

477

15.3.4 Foreline Vent Valve

478

15.3.5 Roughing Pump

478

15.3.7 Battery Charger

478

15.3.8 Power Supply

479

15.3.9 Communications

479

15 - 6

480

15 - 7

481

Figure 15-5 Status Icon

481

15 - 8

482

15 - 9

483

Figure 15-8 Configure Window

483

15 - 10

484

15 - 11

485

15 - 12

486

15 - 14

488

Front Panel Controls

489

15 - 16

490

15.8 Detaching the HAPSITE

491

15 - 18

492

15 - 19

493

15 - 20

494

15 - 21

495

15 - 22

496

15 - 23

497

15 - 24

498

16.1 Introduction

499

16.2 Safety Considerations

500

Symptom Cause Remedy

501

16 - 4

502

16 - 6

504

16.5 Contamination

505

16 - 8

506

C when decontaminating a

506

16 - 9

507

16 - 10

508

16 - 11

509

Figure 16-5 Plugs and Caps

509

16 - 12

510

16 - 13

511

16 - 16

514

16 - 17

515

Figure 16-15 Service Window

516

16 - 19

517

Figure 16-17 Service Window

518

16 - 21

519

16 - 22

520

16 - 23

521

16 - 24

522

6 Remove chain clamp

523

7 Pull the NEG Pump out

523

16 - 26

524

16 - 27

525

16 - 28

526

16 - 29

527

16 - 30

528

16 - 32

530

16 - 33

531

Figure 16-34 Old NEG Pump

531

Figure 16-35 Plus IQ Icon

532

16 - 35

533

16 - 36

534

See Figure 16-42

535

16 - 38

536

16 - 39

537

Figure 16-45 Short Tune Icon

537

16 - 40

538

16 - 41

539

Figure 16-50 Ionizer

542

16 - 45

543

16 - 50

548

17.1 Glossary

549

17 - 2

550

17 - 3

551

17 - 4

552

17 - 5

553

17 - 6

554

17 - 7

555

17 - 8

556

17 - 9

557

17 - 10

558

17 - 11

559

17 - 12

560

Chapter 18

561

Customer Support

561

18 - 2

562

Chapter 19

563

Part Numbers

563

19 - 2

564

19 - 3

565

19.5 Headspace Spare Parts

566

19 - 5

567

19 - 6

568

Appendix A

569

HAPSITE Target Compounds

569

L. This corresponds to

576

C.1 Introduction

577

C.2 Shipping the Canisters

577

Index - 1

581




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